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Papers (1873, 1892-2009, undated) concerning Littleton Female College (later called Littleton College) in Warren County, North Carolina, and its alumnae include correspondence, programs, college history, alumnae lists, clippings, pamphlets and speeches, etc. The college opened in 1882 and closed after a disastrous fire in 1919. The Littleton College Memorial Association was founded in 1926.

Collection (1939) consisting of a pamphlet entitled Bishop[Thomas Campbell] Darst and East Carolina during the past twenty five years [1914-1939]. by Frederick Arthur Turner.

Collection (1899-2004) of printed materials compiled for the centennial of the Orville & Wilbur Wright's first flight at Kitty Hawk, North Carolina; including an article written by the Wright brothers on their flight experiments with various airplanes coupled with printed copies of photographs and a printed reproduction of the article; also copies of Monthly Weather Review magazines from August-September 1899; and a copy of the North Carolina Literary Review dedicated to commemorating the centennial of the first flight complete with poetry and interviews; also two calendars illustrated with images of the Wright brothers flight experiments.

Papers (1822 [1849]-1898) including typewritten transcript, copy, letters, sketches, grade school reports.

Papers (1851-1887) consisting of a memoir, correspondence, legal papers, transcripts, military documents, genealogical materials, and photographic scans pertaining to William Henry von Eberstein (1821- ca. 1890). Descending from German and English aristocracy, he was born in St. Servan, France, and also lived on the Isle of Guernsey before becoming a mariner at age 13. A mariner, soldier, and farmer, von Eberstein moved to Chocowinity, Beaufort County, North Carolina, in 1851 and established himself in business. Later he captained various ships out of Washington, North Carolina, and served in the Confederate army.

The papers and audiovisual materials of Dr. Karen Baldwin, a professor of English and Folklore at ECU.

Collection includes a letter written by Ann Elizabeth Bogart, Washington, N.C., to "My dear Aunt," January 8, 1865, describing wartime conditions in Washington, N.C., and vicinity, a 2-page partial transcription of the letter, a tintype of a woman (possibly Ann Elizabeth Bogart), and two color images of the gravestone for Ann Bogart and the plot where she is buried in Washington, N.C. Also included are research materials concerning David Nevius Bogart of Washington, N.C., and related to the Bogart, Biggs, O'Cain, Lucas, Bonner, Peyton, and Snoad families of Beaufort County, N.C. Photographs, genealogy notes, Bible records, and correspondence relate to the Smallwood, Williams, and Hassell families of Williamston, N.C. Letters related to brothers Will and Bruce Smallwood discuss Will's travels and death (1918) in Alaska and Bruce's life and death (after 1894) in Mexico.

Papers (1904-2009) including correspondence, clippings, programs, magazine, photographs, sermons, and ephemera related to the career of Rev. Cuthbert Warner Bates of the North Carolina Methodist Protestant Church Conference.

Various unrelated items (1862-1865) concerning the Civil War including two 1862 letters, an 1865 oath of allegiance, Harper's Weekly lithographs (1862), an Atlantic and North Carolina Railroad Company 1862 statement, an 1862 $1000 Civil War bond from North Carolina;, and photocopies of a memoir written about fifty years after the war and transcribed in 1978, an 1862 letter and an 1863 circular.

Letterbooks (1864-1866, 1868) including correspondence, letterbooks of handwritten copies of letters, one speech, one cash book, one invoice book, one monthly statement book, one order book, two poems.

Papers (1949-1965), including correspondence, clippings/ reviews, researches notes, historical articles, and miscellaneous.

Civil War Correspondence, (1861–1863) of Union soldier George H. S. Driver, reflecting service in New Bern and Pamlico Sound area of N.C.

Papers (1941-1945) consisting of correspondence, newspaper clippings, photographs, letters and miscellaneous.

This collection consists of the records of the Institute of Outdoor Theatre which was founded in 1963 and includes material related to over 600 outdoor theatres, some of which began operation in the 1920s. Included are play scripts, correspondence, clippings, publicity material, video and audio recordings, feasibility studies, publications, reel-to-reel tapes, 35 mm slides, blueprints, and audition-related materials. This collection is being processed with the support of a National Historical Publications and Records Commission grant.

Items (1928-1941) related to Greenville, NC, resident James Howard Moye; and items (1955) related U.S. Coast Guard rescues in North Carolina. The Zion's Landmark Vol. 23, No. 7 and Vol. 32, No. 7 (10/15/1890 and 2/15/1899) periodical published semi-monthly by Zion's Landmark Print, Wilson, North Carolina (Primitive, or Old School Baptist) that was in the collection has since been transferred to the North Carolina Collection as of 2022.