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"An Accurate Map of North and South Carolina with Their Indian Frontiers" by Henry Mouzon, first published in 1775. Created from detailed surveys conducted by Mouzon and others, the map offers a comprehensive depiction of the geographical and political landscape of the Carolinas prior to the American Revolution. It includes natural features such as mountains, rivers, swamps, and coastal soundings, along with manmade elements like roads, Indian paths, townships, and provincial boundaries. Widely regarded as one of the most authoritative maps of the region during the period, it was used extensively by both British and American forces during the Revolutionary War.

Journal written by Judge Asa Biggs from 1858-1872.

This collection (1961-1999) contains reports, publication issues, newsletter issues, memos, statements, press releases, and a policy guide received by Carroll Webber during his time as a member and as president of the Pitt/Greenville Chapter of the American Civil Liberties Union of North Carolina. Also included are the first four issues of the ACLU "Stand" Magazine (2014-2015).

Collection (1901-1926) of correspondence received by Maud Smith (née Tyson) and her husband Walter Edward "Edd" Smith, from family and friends. Collection includes letters to Maud Tyson, while she attended Littleton Female College, letters from Carl Tyson, during World War I, from the Headquarters of the 81st Division, at Camp Jackson, South Carolina, between May and November, 1918, and several other letters, as well as a list of transcripts and typed transcripts of all letters in the collection.

Collection (1860-1862) including diary, news reports, notes on troop movements, personal experiences relating to friend.

Papers (1921-1955, undated) including orders, reports, memorandums, photographs, scrapbooks, correspondence, pamphlets, clippings, and miscellany.

Papers (1911-1912, 1923, 1939-1950) including correspondence, reports, instructions, handbooks, clippings, photographs, and miscellaneous.

Papers (1923-1986) including correspondence, orders, reports, newsletters, photographs, news clippings, scrapbooks, programs and miscellany.

Partial casualty report (7/6/1863) for the 5th North Carolina Infantry at the Battle of Gettysburg 1 - 3 July 1863, missing pages 1 - 4, but recording the wounded of part of Company G, all of companies H, and K, and including a complete recapitulation of the regiment's losses: killed (39), wounded (235), and missing (55), signed by 2d Lt. Edward S. Smedes who was later killed in action at Spotsylvania Court House, VA.

Includes a public health nursing poem.

The Herman H. Duncan Collection consists of seven photographic prints (1921–1922, undated) depicting Greenville High School athletic teams and unidentified baseball teams in eastern North Carolina. Included are group portraits of the football, basketball, track and field, and baseball teams from Greenville High School, as well as images of unidentified teams, one possibly from New Bern, North Carolina. The photographs document early 20th-century high school athletics and local sports culture in Pitt County and surrounding areas.

Collection (1760-1965) consisting of financial and legal documents, correspondence, genealogical material, a scrapbook, newspapers clippings, photographs, reports.

Papers (1882-1954, undated [bulk 1882-1920]) of U. S. Navy surgeon, including correspondence, reports, and miscellany.

Papers (1944-1945) including correspondence, incoming and outgoing intelligence logbooks, financial reports, orders and a travel account and miscellany.

Papers (1870, 1919-1974) of the U.S. Navy officer, including correspondence, photographs, reports, clippings, certificates, and miscellaneous materials.