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This collection contains materials and documents (1893–1990s) relating to the history of Pitt County, North Carolina Schools, highlighting especially the era of segregation. Includes Registers (1893-1920); football pamphlets (1969–1978) for J.H. Rose High School; Statement of Funds Needed Provided by Pitt County for both "Colored" and "White" schools (1916-1917); a letter (1924) from G.R. Whitfield, Supervisor for "Colored" schools; scrapbooks, scrapbook materials, and news clippings (1970s–1990s) for Third Street School, C.M. Eppes, Greenville Middle School, Agnes Fullilove School and other Pitt County schools; building specifications (1968-1973) related to Pitt County Schools; John Edwin Scoville Memorial Cups (1923-1928).

The Phoenix Historical Society: African American History of Edgecombe County was founded in 2001 to recover, record, and promote the unique history of Edgecombe County (North Carolina) as experienced by members of its African American community. This collection contains the society's official records, brochures, event programs, and publications related to research, community events and sponsored projects.

Papers (1830-1931) including correspondence, speeches, property records, deeds, appointments, clippings, financial records, etc. of a Quaker farmer and business leader in Belvedere (NC).

This collection contains the personal and administrative records of Dr. Otto Henry, a former East Carolina University music professor. Many of the materials pertain to his time at East Carolina although there are also papers from his time as a student at Tulane University and teaching at Washington and Jefferson University.

Collection includes a letter written by Ann Elizabeth Bogart, Washington, N.C., to "My dear Aunt," January 8, 1865, describing wartime conditions in Washington, N.C., and vicinity, a 2-page partial transcription of the letter, a tintype of a woman (possibly Ann Elizabeth Bogart), and two color images of the gravestone for Ann Bogart and the plot where she is buried in Washington, N.C. Also included are research materials concerning David Nevius Bogart of Washington, N.C., and related to the Bogart, Biggs, O'Cain, Lucas, Bonner, Peyton, and Snoad families of Beaufort County, N.C. Photographs, genealogy notes, Bible records, and correspondence relate to the Smallwood, Williams, and Hassell families of Williamston, N.C. Letters related to brothers Will and Bruce Smallwood discuss Will's travels and death (1918) in Alaska and Bruce's life and death (after 1894) in Mexico.