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The Insurance Survey of Greenville collection contains a letter (December 31, 1937) and an insurance survey (December 27, 1937) of the city of Greenville, North Carolina.

Manifest duplicate (15 December 1794) of the Sloop Agnes, bound from Edenton, North Carolina, to New York, New York, carrying barrels of tar, turpentine, and pitch, Thomas Hunter and William Williams, shippers.

This collection contains a journal (December 15, 1861-April 15, 1865) kept by Isaac Liscomb, Master (Commander) of the U.S. Brig Dragoon. Dragoon was a private merchant vessel (formerly called the Remington) leased or purchased by the Union Army for use in the Civil War. As part of General Burnside's fleet, the Dragoon was involved in the Battle of Roanoke Island. Liscomb kept detailed accounts of that battle and of the voyages the ship made during the Civil War to transport troops and supplies to ports including Port Royal and Folly Island (SC), Pensacola (FL), and Morehead City (NC).

Papers (ca. 1867-2007, undated) including photographic negatives, prints, slides and manuscript materials; also video cassettes and moving picture film reels produced during his career as a professional photographer for the Greenville Daily Reflector newspaper, 1952-1972; as bureau chief for the Raleigh News and Observer in Eastern North Carolina; and as news director for television stations WITN-TV, WNCT-TV, 1972-1997; also including personal materials relating to his family and to William W. Speight.

Items (1928-1941) related to Greenville, NC, resident James Howard Moye; and items (1955) related U.S. Coast Guard rescues in North Carolina. The Zion's Landmark Vol. 23, No. 7 and Vol. 32, No. 7 (10/15/1890 and 2/15/1899) periodical published semi-monthly by Zion's Landmark Print, Wilson, North Carolina (Primitive, or Old School Baptist) that was in the collection has since been transferred to the North Carolina Collection as of 2022.

John L. Wooten's daily physician log from 1962.

This collection contains a journal (November 21, 1894 – February 28, 1896) kept by Gilbert Smith Galbraith while he was serving as a U.S. Naval Cadet on board the USS Columbia. The USS Columbia was a Second Line Cruiser first commissioned on April 23, 1894, serving in the U.S. Navy until it was sold for scrap on January 23, 1922. Galbraith includes detailed technical descriptions of the ship and its components along with diagrams, blueprints, scale plans, maps, photographic prints, cyanotypes and various ephemera. Additionally, Galbraith records the ship's activities from November 21, 1894, to February 28, 1896.

Peart's Journal : Prepared from notes kept on a prisoner of War odyssey from Bilibid Prison, Manila, P.I., to Manchukuo, via the prison ship S.S. Oryoku Maru (undated)

Collection contains Greenville and Pitt County, North Carolina, related photographs and ephemera (1917-2007) concerning the Pickwick Book Club, Girl Scouts, Greenville High School, and the Greenville Rotary Club, as well as documents commending the 7th Division American Expeditionary Force for their service in World War I. A large portion of the collection relates to the genealogy of the Goree, Kittrell, Hardee/Hardy, Tull, Proctor, and Hinton families, especially in Eastern North Carolina.

Papers (1944-1998, undated) of Matthew T. Lewis, teacher in Pitt County, N.C., schools and principal of Stokes Elementary School, a segregated, predominantly African American public school in Stokes, Pitt County, North Carolina, including correspondence with the Pitt County Superintendent Arthur S. Alford, announcements of retirement, newspaper clippings, programs from the dedication of Matthew Lewis Field and Picnic Shelter, reports, photographic prints and photograph albums.

Diary and military records of Carter Berkeley Simpson (1915-1944). Includes a typescript of a diary and a facsimile of the diary. The facsimile includes photographs, military records, receipts of letters, correspondence, and a description of daily routine activities during Simpson's service and as a prisoner of war.

This collection (ca. 1909-2002) contains documents related to the career of David Jordan Whichard II of Greenville, N.C., longtime editor of The Daily Reflector and president and chief executive officer of the newspaper's publishing firm. Whichard also served on many professional boards such as the Southern Newspaper Publishers Association, the N.C. Press Association, the Associated Press Board of Directors, the UNC-Chapel Hill Board of Trustees, the ECU Board of Trustees, the UNC System Board of Governors, and on the board for Wachovia Corporation. All of these activities plus other business-related and civic-related activities are reflected in the correspondence, minutes, reports, publications, financial records, and clippings in this collection.

Papers (1894-1914) consisting of letters press book of correspondence and another of financial papers.

Records (1927-2012) including photographic slides & compact discs illustrating City of Greenville Police Department public relations, detective squad, and traffic control operations, including inspections, personnel, court and trail procedures, training programs, including first aid training, bomb disposal, and riot training; also including a letter from Stuart Savage, Senior Writer, The Daily Reflector; to Sergeant Joe Friday & 2 compact discs containing reproductions of black and white and color slides of police operations.

Issue No. LXXIX (1/13/1790) of the Gazette of the United States newspaper containing the announcement of the Adoption and Ratification of the Constitution of the United States by the State of North Carolina, signed in type by President George Washington, p.313-316, (4 p.), published by John Fenno, New York, and autographed "[Moses] Ogden."