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This collection contains materials belonging to alumnus Eva Belle Outlaw, specifically photographs, printed materials, and her 1919 diploma.

This collection (1980s-2010s) contains material related to the life of Michael J. Hamer, an English professor at East Carolina University in Greenville, North Carolina, from 1986 through 2013, and a prolific songwriter, singer, and band leader who died in 2017. Included are notebooks containing his handwritten lyrics, poems, photographs, reel to reel tapes, clippings, and other material pertaining to his musical career.

Collection (1852-2014) includes correspondence, newspaper clippings, printed materials, and other items compiled by retired East Carolina University English professor emeritus Dr. Ralph Hardee Rives (1930-2016) relating primarily to the Hardee - Rives and related families of North Carolina and the United Kingdom, the history of Eastern North Carolina (especially Halifax County and the town of Enfield), the United Methodist Church in Eastern North Carolina, state and local and national politics, and his charitable and philanthropic interests. The earliest original documents cover the period from 1852 through the Civil War and World War I.

Diploma for Charles B. Walton from the Baltimore College of Physicians and Surgeons.

This collection consists of reel-to-reel audiotape footage of U.S. forces at Phan Rang Air Force Base or Da Nang Air Base, South Vietnam, being overrun by Viet Cong attackers. The tape was recorded by Leonard D. Sawyer, Sr., while he was an Avionic Inertial & Radar Nav. Sys. Tech. on a USAF plane during the Vietnam War. Also included is a two-page summary of Mr. Sawyer's service record with the USAF (April 16, 1968 – July 31, 1972).

This collection contains materials (1940s-2013) related to the interests and activities of Holley Mack Bell II and Clara Bond Bell of Windsor and Eden House in Bertie County, N.C. Mr. Bell served in World War II, worked on several newspapers including the Charlotte News, Bertie Ledger-Advance, and the Greensboro Daily News; and was employed by the U.S. Information Agency as a press attaché at several American embassies in South America. Mrs. Bell worked as a social worker, in Public Welfare, and also with social service organizations while they lived in various South American countries. Both Mr. and Mrs. Bell were active in historic preservation, especially with the Historic Hope Foundation, Friends of Hope Committee, Preservation North Carolina, the Museum of the Albemarle, and the Historic Albemarle Tour (HAT), and were active in the Episcopal Church. Included are Bertie Ledger-Advance newspapers, correspondence, publications, photographs, clippings, pamphlets, notes, and brochures.

Papers (1937, undated) including a typescript volume, newspaper clippings, scripts of radio broadcast, African American spirituals.

Papers (1864-1866) of soldier from Beaufort County who was killed in action near Petersburg, Va., during the Civil War while serving in the 33 Regiment of N.C. Troops, including correspondence, especially one notifying his mother of his death.

Papers (1942-1947) include correspondence related to the World War II U.S. Navy careers of Frank A. Bartimo and his brother-in-law Richard Toomey, and Bartimo's civilian life with the Army's Judge Advocate section stationed in post-war Heidelberg, Germany.

Papers include Joseph B. Philips record book, Walter E. Philips' memoirs, poems and other writings, and biographical information about several Philips men.

Papers (1854-1865) including typescripts, correspondence, photocopies of army muster rolls, enlistment contract and discharge, letters comment on destruction of standing crops of Virginia, the demolition of Hampton, etc.

This collection consists of 48 deeds (1801-1907), legal documents and notes related to land ownership in Pitt County, North Carolina, in the area that became Ayden. The documents pertain mainly to the Harris, McGlohon/McLawhorn, and Cannon families, especially William Henry Harris, the founder of Ayden. Also included are a blueprint plat of Ayden (June 21, 1890) and copies of 2 clippings (1991-1992) about the founding of Ayden. Additional items which have been placed in the East Carolina University Archives are a 1915 yearbook for East Carolina Teachers Training School (now ECU), a 1915 folded card for the Junior-Senior Reception at ECTTS, and a calling card all belonging to ECTTS student Katherine (Kate or Katie) Eugenia Sawyer. This collection is donated by the family of John William Sawyer.

The collection includes publications created by the ECU School of Medicine and the University Health Systems of Eastern Carolina, formerly Pitt County Memorial Hospital.

Journal of a Cruize in the USS Independence, Commodore William Bainbridge's Flag Ship, Capt. William M. Crane, Commander, from Boston, July 2nd, 1815 (3 July–15 November 1815), compiled by an anonymous crew member, which describes the first overseas mission of the first ship of the line commissioned by the United States Navy, to deal with the piratical acts of the Barbary Powers against American merchant commerce in the Mediterranean Sea, bound in original calf leather over marbled boards, entries clean and legible; also a letter from William M. Crane, Commanding Officer, USS Delaware, Port Mahon (20 September 1829) to Lt. William N, McKean, U.S. sloop Warren, ordering him to report to Lt. Thomas M. Newell, commander of the U.S. schooner Porpoise.