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Papers (1743 – 1985) of the descendants of Martin Whitford and Nancy Purifoi (Purifoy) Whitford, of Craven County NC, including David Purifoi Whitford, Susan Cox, Addison Purifoi Whitford, Pamela Toler and Edna Whitford Fisher, and consisting of land, legal and business records, genealogical charts and a family history, a photographic print, and the constitutions of the Mt. Lebanon Church and the Broad St. Church & Secondary School 100 Per Cent Loyalty and Service Club.

Collection (1973–1989) of color slides documenting J. Y. Joyner Library at East Carolina University, in October 1973, prior to the construction of two extra floors and the addition of a new west wing to the building, for Library Science 1000 class; also photocopies of correspondence, historical research reports, and newspaper clippings about the Greenville Town Common Confederate flags controversy, in 1983–1989; also photocopies of newspaper clippings about the Confederate flag, 1983–1989. Collection also contains 4 photographs of individuals from the Collins-Becton family.

Collection (1766-2010) consists of items related to the Augustus Moore (June 8, 1803-March 23, 1851) family of Chowan and Halifax Cos., N.C., his children Augustus Minton Moore, William Armistead Moore, Henrietta Moore Sutton, Susan Augustus Moore Righton, Mary Elizabeth Moore, Alfred Moore and John Armistead Moore, and the descendants of John Armistead Moore. Included are account books, legal records, land transactions, estate records, correspondence, clippings, and autograph books (1855, 1865) belonging to family members who attended Miss Willard's Female Seminary in Troy, N.Y., and Patapsco Female Institute in Ellicott City, Maryland. Also included are identified photographs (cartes de visite, tintypes, cased pictures, albums) of the Moore, Gilliam, and Skinner, families, religious books such as Roman Catholic Missals, Episcopal Books of Common Prayer and Bibles, UNC-Chapel Hill diplomas (1824), and items related to the 1878 Exposition in Paris, France.

Diary (Sept. 1943-Dec. 1944) of Joseph John Valinsky, a sailor aboard the USS Monterey, kept during World War II duty in the Pacific, along with correspondence, certificates, and military service identification cards.

This pocket diary was kept by Union soldier James F. Shapleigh of 43rd Massachusetts Volunteers, Co. D, from January 1, 1863, through July 20, 1863. He was mustered out at the end of July 1863. During this period the 43rd Massachusetts Volunteers served in North Carolina with the 1st Brigade, 1st Division, 18th Army Corps. Camp Rogers in New Bern, was home base. Included in the diary are good details related to the Battle of Washington, North Carolina, that covers March 30 to April 19, 1863, as well as everyday life for soldiers. Later scattered entries in the diary go through January 1864.

Collection (1753-1852) including deeds concerning Bladen and Bath counties (NC).

This collection contains materials that date from Dowell's time as a student at East Carolina Teachers Training school and her subsequent teaching career. It contains awards received from both civic and professional organizations, clippings, personal artifacts, and scholarly works including her Masters Thesis.

Genealogical materials given by Martha Mewborn Marble including Bible records, photographs, notes, legal documents, land records, and clippings concerning families in Greene, Lenoir, Jones, and Pitt counties, North Carolina. Some of the families included are Mewborn, Kilpatrick, Albritton, Pugh, Cannon, Batchelor, Howell, Ormond, Carr, Hardison, Taylor, Sutton, Jackson, Frye, Ham, Hartsfield, Dupree, Faulkner, Rouse, Phillips, Franklin, Joyner, Bryan, Hatch, Cox, McCoy, and Abbott families. Also included are Le-Nea, the first yearbook (1938) for Contentnea High School, Graingers, Lenoir County, North Carolina, autograph books, and a ledger (1888-1892) of Wilbar General Store, Greenville, Pitt County, North Carolina. The Kayaitchess (1924) Vol. 1, published by the students of Kinston High School, Kinston, North Carolina, and the Connecting Link Commencement Issue 1926, published every other week by students of Kinston City Schools under the Supervision of Committee of Teachers have been transferred to the North Carolina Collection and have been catalogued.

Collection includes a letter written by Ann Elizabeth Bogart, Washington, N.C., to "My dear Aunt," January 8, 1865, describing wartime conditions in Washington, N.C., and vicinity, a 2-page partial transcription of the letter, a tintype of a woman (possibly Ann Elizabeth Bogart), and two color images of the gravestone for Ann Bogart and the plot where she is buried in Washington, N.C. Also included are research materials concerning David Nevius Bogart of Washington, N.C., and related to the Bogart, Biggs, O'Cain, Lucas, Bonner, Peyton, and Snoad families of Beaufort County, N.C. Photographs, genealogy notes, Bible records, and correspondence relate to the Smallwood, Williams, and Hassell families of Williamston, N.C. Letters related to brothers Will and Bruce Smallwood discuss Will's travels and death (1918) in Alaska and Bruce's life and death (after 1894) in Mexico.

Papers, certificates, photos, and artifacts of Dr. Edwin Wall Monroe. This collection contains a great deal of information regarding the development of the East Carolina School of Medicine, including planning, politics, legislation, advertisement, construction, partnerships, details of the personnel involved, groundbreakings and other ceremonies, departments, additional buildings, and community services.

George Vernon Holloman was born in Rich Square, North Carolina on September 17, 1902. This collection deals with the last years of his career in the U.S. Army Air Corps in 1945-1946. He was a colonel and very involved in developing advanced technologies related to automatic landing and flying systems in the Air Technical Service Command (ATSC) at Wright Field. While on duty with the 20th Air Force in Guam as deputy chief of staff, he died in a plane crash over Formosa. Included are clippings, photographs and a postcard.

This candid and detailed World War I diary (April 25, 1918-March 12, 1919) was kept by Carl Whittlesey of Barton County, MO, during his service with the 313 Engineers 88th Division. He kept detailed entries regarding his training at Camp Dodge in Johnston, Iowa, his participation in the Alsace Campaign in France, and his involvement in developing the war ravaged areas in Europe.

Record (1902-1967) consisting of correspondence, tobacco records, financial and business papers, ledger, etc.

This collection contains the congressional files for U.S. House of Representatives member Walter B. Jones, Jr., who represented the 3rd Congressional District of North Carolina from 1995 until his death in 2019. Included are files, scrapbooks, media, and electronic files. The electronic files were created by his staff and included speeches, correspondence, articles, promotional material, notes and videos for the years 2005-2018.

The Phoenix Historical Society: African American History of Edgecombe County was founded in 2001 to recover, record, and promote the unique history of Edgecombe County (North Carolina) as experienced by members of its African American community. This collection contains the society's official records, brochures, event programs, and publications related to research, community events and sponsored projects.